Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → 6H-oxazolo[4,5-e]indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | 5-Hydroxyindole | HCID 16054 | — |
| 촉매 | Manganese dioxide | HCID 14801 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 6H-oxazolo[4,5-e]indole | HCID 11332609 | — |
반응 단계
0.5 mmol of methylamine and 4.13 mmol of MnO2 are added to a solution of 0.4 mmol of 5-hydroxy-1H-indole in 3 ml of DMF, and the mixture is stirred at room temperature for 18 hours. The suspension is filtered through Celite and subjected to conventional work-up, giving 6H-oxazolo[4,5-e]indole; ESI 159.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741343B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-48e2ebd3ce31455ea6dd59c9383f0a06 |
| 출처 메모 | uspto-grants-2010_06 |