Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Dichlorobenzene → 7-Allyl-1H-indazol-6-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 반응물 | 6-Allyloxy-1H-indazole | HCID 22496569 | — |
| 생성물 | 7-Allyl-1H-indazol-6-ol | HCID 135843647 | 60% |
반응 단계
A solution of the product from Step A (14.2 g, 82 mmol) in 1,2-dichlorobenzene (90 mL) was fluxed for 6 h and the reaction mixture was evaporated to a residue which was purified by chromatography (silica, EtOAc) to give a tan solid (8.59 g, 60%) that was used in the next step: LC/MS (+APCI) m/z 175 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06881749B2 |
| 출처 데이터셋 | uspto-grants-2005_04 |
| ORD ID | ord-36faabe96ce14c83ab09362c11ff1eb9 |
| 출처 메모 | uspto-grants-2005_04 |