Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methoxypropylamine → (7-Bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methoxypropylamine | HCID 1672 | — |
| 반응물 | 7-Bromo-4-chloro-3-nitroquinoline | HCID 21984361 | — |
| 생성물 | (7-Bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine | HCID 21984327 | 94.2% |
반응 단계
7-Bromo-4-chloro-3-nitroquinoline (29.54 g, 102.7 mmol) was reacted with 3-methoxy propyl amine (10.07 g, 113.0 mmol) according to the method described in Part A of Examples 125-135 to provide 32.9 g of (7-bromo-3-nitroquinolin-4-yl)-(3-methoxypropyl)amine as a yellow solid. The product was not recrystallized.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07598382B2 |
| 출처 데이터셋 | uspto-grants-2009_10 |
| ORD ID | ord-0577e3a026534b0f825b9a02214d4dce |
| 출처 메모 | uspto-grants-2009_10 |