1-Methylimidazole → 1-Methyl-3-5-hexenyl imidazolium chloride

HRID 1819516

반응식

HRID 1819516 반응식
[Cl:1][CH2:2][CH2:3][CH2:4][CH2:5][CH:6]=[CH2:7].[CH3:8][N:9]1[CH:13]=[CH:12][N:11]=[CH:10]1>>[Cl-:1].[CH3:8][N+:9]1[CH:13]=[CH:12][N:11]([CH2:2][CH2:3][CH2:4][CH2:5][CH:6]=[CH2:7])[CH:10]=1

참가 물질

3

반응물 2

HCID 13901-MethylimidazoleHCID 702336-Chloro-1-hexene

생성물 1

HCID 866135771-Methyl-3-5-hexenyl imidazolium chloride

실험 절차

The procedure of Example 1 was repeated with minor changes. 51.0 g of 6-chloro-1-hexene (Aldrich) and 35.3 g of 1-methylimidazole (Aldrich) were added into a 2000 ml three-neck round-bottom flask. The reaction temperature was set from 75 to 80° C. After four hours the milk-like solution transferred into a homogenous solution. The reaction was continued for three days. Then, the product was washed with ethyl acetate five times. After that, it was dried under vacuum for three days.

후처리

  1. customwas set from 75 to 80° C
  2. waitThe reaction was continued for three days
  3. washThen, the product was washed with ethyl acetate five times
  4. customAfter that, it was dried under vacuum for three days

출처 및 근거

ORD 기록
ord-49914fd29db940af8f0829468a36a0ae
출처 데이터셋
uspto-grants-2009_10
특허 번호
US07601772B2

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