참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 4-Amino-2,5-dimethylphenol | HCID 76544 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Acetamide, N-(4-hydroxy-2,5-dimethylphenyl)- | HCID 155307 | 90.4% |
반응 단계
To a suspension of 4-amino-2,5-dimethyl-phenol (6.85 g, 50 mmol) in 30 mL of water was added acetic anhydride (5.67 mL, 60 mmol). The mixture was vigorously stirred at 70° C. for 20 min and then cooled down to room temperature. The solid was collected by filtration and washed with water to give N-(4-hydroxy-2,5-dimethyl-phenyl)-acetamide as gray solid (8.1 g, 90%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07037909B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_05 |
|---|
| ORD ID | ord-319565c3bd714555a2d8cd31a5c25312 |
|---|
| 출처 메모 | uspto-grants-2006_05 |
|---|
