Tributylamine → 5-Butoxy-4-methyl-1,3-oxazole

HRID 1823338

반응식

HRID 1823338 반응식
[N+:1]([CH:3]([CH3:11])[C:4]([O:6][CH2:7][CH2:8][CH2:9][CH3:10])=[O:5])#[C-:2].C(N(CCCC)CCCC)CCC>ClC1C=CC=CC=1>[CH3:11][C:3]1[N:1]=[CH:2][O:5][C:4]=1[O:6][CH2:7][CH2:8][CH2:9][CH3:10]

참가 물질

4

반응물 2

HCID 7622TributylamineHCID 11171108n-Butyl alpha-isocyanopropionate

생성물 1

HCID 98774405-Butoxy-4-methyl-1,3-oxazole

시약·촉매·용매 1

HCID 7964Chlorobenzene용매

실험 절차

A continuously operated dividing wall column (4.8 m×64 mm) packed with 3×3 mm V2A Raschig rings and a dividing wall of height 2.4 m having 60 theoretical plates was charged with a mixture of 13.1% by weight of n-butyl α-isocyanopropionate (R1=n-butyl, R2=methyl), 32.2% by weight of monochlorobenzene and 50.1% by weight of tri-n-butylamine.

출처 및 근거

ORD 기록
ord-5d92cae410694a43864bb8ca79139d29
출처 데이터셋
uspto-grants-2006_05
특허 번호
US07038058B2

연결된 노트

불러오는 중…