3-(2,4-Dichlorophenyl)-2,5-dimethylpyrazine 1-oxide → 3-(2,4-Dichlorophenyl)-2,5-diethylpyrazine 1-oxide

HRID 1824065노트

반응식

HRID 1824065 반응식
ClC1C=C(Cl)C=CC=1C1C(C)=[N+]([O-:16])C=C(C)N=1.[Cl:18][C:19]1[CH:24]=[C:23]([Cl:25])[CH:22]=[CH:21][C:20]=1[C:26]1[C:27]([CH2:34][CH3:35])=[N:28][CH:29]=[C:30]([CH2:32][CH3:33])[N:31]=1>>[Cl:18][C:19]1[CH:24]=[C:23]([Cl:25])[CH:22]=[CH:21][C:20]=1[C:26]1[C:27]([CH2:34][CH3:35])=[N+:28]([O-:16])[CH:29]=[C:30]([CH2:32][CH3:33])[N:31]=1

참가 물질

3

반응물 2

HCID 221472913-(2,4-Dichlorophenyl)-2,5-dimethylpyrazine 1-oxideHCID 221473543-(2,4-Dichlorophenyl)-2,5-diethylpyrazine

생성물 1

HCID 221472153-(2,4-Dichlorophenyl)-2,5-diethylpyrazine 1-oxide

실험 절차

Following the procedure of 3-(2,4-dichlorophenyl)-2,5-dimethylpyrazine 1-oxide but substituting Preparation of 3-(2,4-dichlorophenyl)-2,5-diethylpyrazine and making non-critical variations, the title compound was obtained (quantitative). It was used without preparation. 1H NMR (CDCl3) δ 1.12, 1.34, 2.55, 2.81, 2.89, 7.28, 7.40, 7.55, 8.11.

출처 및 근거

ORD 기록
ord-ba7de50a3d5c4d2dbf25952660843260
출처 데이터셋
uspto-grants-2006_05
특허 번호
US07041672B2

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