Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine → 4-Piperidinylbut-1-ene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | Homoallyl bromide | HCID 21241 | — |
| 생성물 | 4-Piperidinylbut-1-ene | HCID 4562282 | 93.4% |
반응 단계
4-Bromobut-1-ene (1.35 g) was treated with piperidine (1.7 g) and heated at reflux for 3 hours. The mixture was cooled to ambient temperature, filtered and the residue washed with ether (50 mL). The combined filtrate and washings were evaporated to give the title compound (1.3 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07041827B2 |
| 출처 데이터셋 | uspto-grants-2006_05 |
| ORD ID | ord-adb29397f4884d54a3b13354f001a0f2 |
| 출처 메모 | uspto-grants-2006_05 |