p-Cyanobenzenesulphonamide → 4-cyano-N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamide

참여 물질

역할	이름	HCID	투입량
반응물	p-Cyanobenzenesulphonamide	HCID 76566	—
반응물	3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid	HCID 3036152	—
생성물	4-cyano-N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-benzenesulfonamide	HCID 69781487	—

반응 단계

Prepared by coupling 1a and 4-cyanobenzenesulfonamide in accordance with Procedure 1, Method B described hereinabove. Yield (21%); 1H NMR (d6-DMSO) δ 8.09–8.03 (m, 4H), 7.94 (d, J=8.0 Hz, 1H), 7.40–7.07 (m, 12H), 6.84 (d, J=8.0 Hz, 2H), 6.40 (d, J=15.7 Hz, 1H), 2.35 (q, J=7.4 Hz, 2H), 0.82 (t, J=7.4 Hz, 3H); APcI m/z: 519 (M+H+).

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US07045540B2
출처 데이터셋	uspto-grants-2006_05
ORD ID	ord-5e33c4f5736f4876991d1d07c2c1209e
출처 메모	uspto-grants-2006_05