Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl indole-2-carboxylate → 4-fluoro-1-methyl-1H-indole-3-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl indole-2-carboxylate | HCID 73125 | — |
| 반응물 | 4-Fluoro-1H-indole-3-carbaldehyde | HCID 22139006 | — |
| 생성물 | 4-fluoro-1-methyl-1H-indole-3-carbaldehyde | HCID 22138994 | 54% |
반응 단계
According to the procedure of Preparation 9 (a), except substituting 4-fluoro-1H-indole-3-carboxaldehyde (0.41 g, 2.5 mmole) for the ethyl-indole-2-carboxylate, the title compound (0.24 g, 54%) was prepared as a viscous oil: MS (ES) m/e 178 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741339B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-d928788cda6740eb8747d4e943ef233e |
| 출처 메모 | uspto-grants-2010_06 |