1-Nitro-4-{[4-(trifluoromethyl)benzyl]oxy}benzene → 4-(4-Trifluoromethyl-benzyloxy)-phenylamine

HRID 1827378

반응식

HRID 1827378 반응식
FC1C=C(C=CC=1)COC1C=CC(N)=CC=1.[F:17][C:18]([F:37])([F:36])[C:19]1[CH:35]=[CH:34][C:22]([CH2:23][O:24][C:25]2[CH:30]=[CH:29][C:28]([N+:31]([O-])=O)=[CH:27][CH:26]=2)=[CH:21][CH:20]=1>>[F:17][C:18]([F:36])([F:37])[C:19]1[CH:35]=[CH:34][C:22]([CH2:23][O:24][C:25]2[CH:30]=[CH:29][C:28]([NH2:31])=[CH:27][CH:26]=2)=[CH:21][CH:20]=1

참가 물질

3

반응물 2

HCID 27437921-Nitro-4-{[4-(trifluoromethyl)benzyl]oxy}benzeneHCID 167753144-(3-Fluoro-benzyloxy)-phenylamine

생성물 1

HCID 221378894-(4-Trifluoromethyl-benzyloxy)-phenylamine수율 98%

실험 절차

Prepared in analogy to 4-(3-fluoro-benzyloxy)-phenylamine, by hydrogenation of 4-(4-trifluoromethyl-benzyloxy)-nitrobenzene. Yield: 98% of a slightly yellow solid. MS: m/e=268.3 (M++H).

출처 및 근거

ORD 기록
ord-94ce0f81d0c84ff09fc837f34ff5c21a
출처 데이터셋
uspto-grants-2006_05
특허 번호
US07053245B2

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