5-Nitrosalicylaldehyde → 2-((3-Fluorobenzyl)oxy)-5-nitrobenzaldehyde

HRID 1827425

반응식

HRID 1827425 반응식
[OH:1][C:2]1[CH:9]=[CH:8][C:7]([N+:10]([O-:12])=[O:11])=[CH:6][C:3]=1[CH:4]=[O:5].[F:13][C:14]1[CH:15]=[C:16]([CH:19]=[CH:20][CH:21]=1)[CH2:17]Br>>[F:13][C:14]1[CH:15]=[C:16]([CH:19]=[CH:20][CH:21]=1)[CH2:17][O:1][C:2]1[CH:9]=[CH:8][C:7]([N+:10]([O-:12])=[O:11])=[CH:6][C:3]=1[CH:4]=[O:5]

참가 물질

3

반응물 2

HCID 668085-NitrosalicylaldehydeHCID 680073-Fluorobenzyl bromide

생성물 1

HCID 27795602-((3-Fluorobenzyl)oxy)-5-nitrobenzaldehyde수율 95%

실험 절차

Prepared in analogy to example 8 from 2-hydroxy-5-nitrobenzaldehyde and 3-fluoro-benzylbromide. Colorless solid. Yield=95%. MS: m/e=275.1 (M+).

출처 및 근거

ORD 기록
ord-c52577e6b9b84038bfff580166e7a30c
출처 데이터셋
uspto-grants-2006_05
특허 번호
US07053245B2

연결된 노트

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