5-Methoxyindole-3-carbaldehyde → 5-methoxy-1-methyl-1H-indole-3-carbaldehyde

HRID 18275

반응식

HRID 18275 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[NH:8][CH:7]=[C:6]2[CH:12]=[O:13].[CH3:14]C1(C=O)C2C(=CC=CC=2)NC1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][CH:11]=1)[N:8]([CH3:14])[CH:7]=[C:6]2[CH:12]=[O:13]

참가 물질

3

반응물 2

HCID 827585-Methoxyindole-3-carbaldehydeHCID 22139118HCID 22139118, 화합물

생성물 1

HCID 9259735-methoxy-1-methyl-1H-indole-3-carbaldehyde수율 92%

실험 절차

According to the procedure of Preparation 13 (a), except substituting 5-methoxy-1H-indole-3-carboxaldehyde for the 3-methyl-1H-indole-3-carboxaldehyde, the title compound (0.86 g, 92%) was obtained as a light tan solid: MS (ES) m/e 190.2 (M+H)+.

출처 및 근거

ORD 기록
ord-016afe0cdf3c4fc392b5782ab1e68d0b
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07741339B2

연결된 노트

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