Methyl 4-(aminomethyl)benzoate → Methyl 4-(acetamidomethyl)benzoate
반응식
[NH2:1][CH2:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([O:9][CH3:10])=[O:8])=[CH:5][CH:4]=1.C(C1(N[C:34]([CH:36](NC(N2CCOCC2)=O)CC(C)(C)C)=[O:35])CC(C2C=CC=CC=2)NC(C2C=CC=CC=2)C1)#N.C(C1(NC(C(NC(N2CCOCC2)=O)CC2CCCCC2)=O)CCN(C)CC1C)#N>C(O)(=O)C>[CH3:10][O:9][C:7](=[O:8])[C:6]1[CH:5]=[CH:4][C:3]([CH2:2][NH:1][C:34](=[O:35])[CH3:36])=[CH:12][CH:11]=1참가 물질
5
반응물 3
생성물 1
시약·촉매·용매 1
실험 절차
Methyl-4-(acetylamino-methyl)-benzoate was prepared from acetic acid and methyl 4-(aminomethyl)benzoate using a method analogous to that of Example 1-part (d). The crude N-acyl ester was saponified using a method analogous to that of Example 1-part (c). The crude product was used without further purification.
후처리
- customThe crude product was used without further purification
출처 및 근거
- ORD 기록
- ord-cdb95c2952dc4cf2ac6968de6e52a013
- 출처 데이터셋
- uspto-grants-2006_06
- 특허 번호
- US07056915B2
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