참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-tert-Butylcyclohexanol | HCID 7391 | — |
| 반응물 | Potassium bisulfate | HCID 516920 | — |
| 반응물 | ethylacetate KHSO4 | HCID 86585043 | — |
| 생성물 | 4-Tert-butylcyclohex-1-ene | HCID 16688 | — |
반응 단계
20 g 4-t-butyl-1-cyclohexanol are mixed with 17 g KHSO4 and stirred for one week at 95° C. After the addition of ethylacetate KHSO4 is filtered off. Ethylacetate is evaporated and the product obtained by fractional distillation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07057059B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_06 |
|---|
| ORD ID | ord-af0b71c7642b4961a781a860d53df6c6 |
|---|
| 출처 메모 | uspto-grants-2006_06 |
|---|
