Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methyl-1H-indole-3-carbaldehyde → HCID 66905063, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methyl-1H-indole-3-carbaldehyde | HCID 87894 | — |
| 반응물 | 2-Chloro-1-methyl-1H-indole-3-carbaldehyde | HCID 314792 | — |
| 생성물 | HCID 66905063 | HCID 66905063 | 90% |
반응 단계
According to the procedure of Preparation 12, except substituting 2-chloro-1-methyl-1H-indole-3-carboxaldehyde (3.0 g, 15.5 mmole) for the 1-methylindole-3-carboxaldehyde, the title compound (2.91 g, 90%) was prepared as an oil: 1H NMR (400 MHz, CDCl3) δ 7.60 (d, J=7.9 Hz, 1 H), 7.22 (m, 2 H), 7.13 (m, 1 H), 3.92 (s, 2 H), 3.71 (s, 3 H), 2.44 (s, 3 H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741339B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-2ae7ea1641db4164a56859ad8f43adb2 |
| 출처 메모 | uspto-grants-2010_06 |