Carbamic chloride, N-methyl-N-phenyl- → HCID 10172359, 화합물

HRID 1831100노트

반응식

HRID 1831100 반응식
[CH2:1]([S:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>>[CH2:1]([S:8][C:9]1[CH:14]=[CH:13][C:12]([O:15][C:18](=[O:19])[N:17]([CH3:16])[C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

참가 물질

3

반응물 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 36142834-(heptylsulfanyl)phenol

생성물 1

HCID 10172359HCID 10172359, 화합물

실험 절차

The title compound was prepared from 4-heptylsulfanyl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (74%, colourless oil, HPLC-MS m/z=358.2 (M+1), Rt: 6.21 min.

출처 및 근거

ORD 기록
ord-5bc081b20b064cc79aaf71675a18a4b8
출처 데이터셋
uspto-grants-2006_06
특허 번호
US07067517B2

반응 노트

불러오는 중…