4-Pentylphenol → Methyl-phenyl-carbamic acid 4-pentyl-phenyl ester

HRID 1831168노트

반응식

HRID 1831168 반응식
[CH2:1]([C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[CH3:13][N:14]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:15](Cl)=[O:16]>>[CH2:1]([C:6]1[CH:7]=[CH:8][C:9]([O:12][C:15](=[O:16])[N:14]([CH3:13])[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH3:5]

참가 물질

3

반응물 2

HCID 269754-PentylphenolHCID 77969Carbamic chloride, N-methyl-N-phenyl-

생성물 1

HCID 69517564Methyl-phenyl-carbamic acid 4-pentyl-phenyl ester

실험 절차

The title product was prepared from 4-pentylphenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (4%, light brown oil). HPLC-MS: m/z=298.2 (M+1); Rt: 5.61 min.

출처 및 근거

ORD 기록
ord-a4c9171dd7b5431b97ed0fd2d72ea8b1
출처 데이터셋
uspto-grants-2006_06
특허 번호
US07067517B2

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