Carbamic chloride, N-methyl-N-phenyl- → HCID 69518123, 화합물

HRID 1831189노트

반응식

HRID 1831189 반응식
[OH:1][C:2]1[CH:16]=[CH:15][C:5]([C:6]([N:8]2[CH2:13][CH2:12][N:11]([CH3:14])[CH2:10][CH2:9]2)=[O:7])=[CH:4][CH:3]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[CH3:14][N:11]1[CH2:10][CH2:9][N:8]([C:6]([C:5]2[CH:15]=[CH:16][C:2]([O:1][C:19](=[O:20])[N:18]([CH3:17])[C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)=[CH:3][CH:4]=2)=[O:7])[CH2:13][CH2:12]1

참가 물질

3

반응물 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 4740811(4-Hydroxyphenyl)(4-methylpiperazin-1-yl)methanone

생성물 1

HCID 69518123HCID 69518123, 화합물

실험 절차

The title product was prepared from 1-(4-hydroxybenzoyl)-4-methyl-piperazine and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (22%, colorless oil). HPLC-MS: m/z=354.1 (M+1); Rt: 2.07 min.

출처 및 근거

ORD 기록
ord-d9a2b7bb13a84bc59d20d25842f360ae
출처 데이터셋
uspto-grants-2006_06
특허 번호
US07067517B2

반응 노트

불러오는 중…