Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-hydroxymethyl-pyrazol-1-yl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| 반응물 | 1-Hydroxy-4-hydroxymethylpyrazole | HCID 22047685 | — |
| 생성물 | Methyl-phenyl-carbamic Acid 4-hydroxymethyl-pyrazol-1-yl Ester | HCID 69517970 | — |
반응 단계
The title compound was prepared from 1-hydroxy-4-hydroxymethylpyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (62%, oil).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07067517B2 |
| 출처 데이터셋 | uspto-grants-2006_06 |
| ORD ID | ord-b88859a656dc439996cc7e400ae7589d |
| 출처 메모 | uspto-grants-2006_06 |