Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Dithionite → 4-(2-chloro-4-trifluoromethyl-phenyl)-N2-(1-methoxymethyl-propyl)-pyridine-2,3-diamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Dithionite | HCID 24489 | — |
| 반응물 | [4-(2-Chloro-4-trifluoromethyl-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine | HCID 22052174 | — |
| 생성물 | 4-(2-chloro-4-trifluoromethyl-phenyl)-N2-(1-methoxymethyl-propyl)-pyridine-2,3-diamine | HCID 69658046 | 78% |
반응 단계
[4-(2-Chloro-4-trifluoromethyl-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine (0.40 g, 1.0 mmol) and Na2S2O4 (1.39 g, 8.0 mmol) were treated substantially as described in Part E of Example 9 to yield 0.29 g (78%) of 4-(2-chloro-4-trifluoromethyl-phenyl)-N2-(1-methoxymethyl-propyl)-pyridine-2,3-diamine: MS (AP) m/z 373.8 [(M+H)+, 100].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07067658B2 |
| 출처 데이터셋 | uspto-grants-2006_06 |
| ORD ID | ord-b7befaffeb084babb4395e25a5026d54 |
| 출처 메모 | uspto-grants-2006_06 |