N-(1-pyridin-4-ylethyl)formamide → HCID 22052374, 화합물

HRID 1831807노트

반응식

HRID 1831807 반응식
[N:1]1[CH:6]=[CH:5][C:4]([CH:7]([NH:9][CH:10]=[O:11])[CH3:8])=[CH:3][CH:2]=1.[H][H]>C(O)(=O)C>[NH:1]1[CH2:6][CH2:5][CH:4]([CH:7]([NH:9][CH:10]=[O:11])[CH3:8])[CH2:3][CH2:2]1

참가 물질

4

반응물 2

HCID 2771720N-(1-pyridin-4-ylethyl)formamideHCID 178418361HCID 178418361, 화합물

생성물 1

HCID 22052374HCID 22052374, 화합물

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

N-(1-Pyridin-4-yl-ethyl)-formamide (1.86 g, 12.38 mmol) was dissolved in 50 ml of acetic acid. After addition of Rh (5% on Al2O3, 307 mg) the mixture was hydrogenated with 10 bar hydrogen and 100° C. for 120 hours. The mixture was evaporated and lyophilised. The crude material was used without purification.

후처리

  1. customThe mixture was evaporated
  2. customThe crude material was used without purification

출처 및 근거

ORD 기록
ord-e9ad8eb38b184374bd02bcba4d2cf473
출처 데이터셋
uspto-grants-2006_06
특허 번호
US07067665B2

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