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Acetic Acid → HCID 54161447, 화합물

HRID 1833396
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인쇄 미리보기

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HRID 1833396 반응식
[CH3:1][O:2][C:3]([C:5]1[NH:6][C:7]2[C:12]([C:13]=1[O:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[N+:21]([O-])=O)=[CH:11][CH:10]=[CH:9][CH:8]=2)=[O:4].C(O)(=O)C>[Fe].C(O)C>[CH3:1][O:2][C:3]([C:5]1[NH:6][C:7]2[C:12]([C:13]=1[O:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[NH2:21])=[CH:11][CH:10]=[CH:9][CH:8]=2)=[O:4]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 2

HCID 176Acetic AcidHCID 54304514Methyl 3-(2-nitrophenoxy)-1H-indole-2-carboxylate

생성물 1

HCID 54161447HCID 54161447, 화합물

시약·촉매·용매 2

HCID 23925Iron촉매HCID 702Ethanol용매

실험 절차

A mixture of 3.12g of methyl-3-[o-nitrophenoxy]-indole-2-carboxylate, 10g of 40 mesh iron filings, 5ml of 5% aqueous acetic acid and 300ml of ethanol was refluxed with stirring for 3 hours. The mixture was filtered and concentrated to a solid. Recrystallization from ethanol gave analytical material, mp. 183°-4°.

후처리

  1. temperaturewas refluxed
  2. filtrationThe mixture was filtered
  3. concentrationconcentrated to a solid
  4. customRecrystallization from ethanol
  5. customgave analytical material, mp. 183°-4°

출처 및 근거

ORD 기록
ord-5164e81c0f134ed5ae9afd1a5b2edfcf
출처 데이터셋
uspto-grants-1978_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04066660

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