Acetone → Ethyl 6-methylnicotinate
반응식
[CH3:1][C:2]1[CH:13]=[CH:12][C:5]([C:6](CC(=O)C)=[O:7])=[CH:4][N:3]=1.[CH3:14][C:15](C)=[O:16]>>[CH2:15]([O:16][C:6]([C:5]1[CH:12]=[CH:13][C:2]([CH3:1])=[N:3][CH:4]=1)=[O:7])[CH3:14]참가 물질
3
실험 절차
The 6-methylnicotinoyl-acetone which is mentioned as the starting substance in Example 6, can be obtained in a known manner from α-picoline-5-carboxylic acid ethyl ester and acetone, or from 5-acetyl-α-picoline (prepared in accordance with Angew. Ch. 67, page 398) and ethyl acetate:
출처 및 근거
- ORD 기록
- ord-7302fab9ec1b477bad43ebb018842f53
- 출처 데이터셋
- uspto-grants-1978_01
- 특허 번호
- US04066768
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