Hydrogen Peroxide → HCID 178460815, 화합물

반응식

[CH2:1](Cl)[CH:2]=[CH2:3].[C:5]([N:7]=[C:8]([S-:10])[S-:9])#[N:6].[K+].[K+].[OH:13]O>>[OH:13][C:5]1[N:7]=[C:8]([S:10][CH2:1][CH:2]=[CH2:3])[S:9][N:6]=1

참가 물질

반응물 3

HCID 784Hydrogen Peroxide

HCID 7850Allyl chloride

HCID 83179Carbamodithioic acid, N-cyano-, potassium salt (1:2)

생성물 1

HCID 178460815HCID 178460815, 화합물

실험 절차

77 g of allyl chloride and 195 g of potassium N-cyanodithioimidocarbonate were condensed and the reaction product was oxidized with 100 ml of 30% hydrogen peroxide to obtain 63 g of 3-hydroxy-5-allylthio-1,2,4-thiadiazole melting at 84° C.

후처리

customcondensed

출처 및 근거

ORD 기록: ord-3325b01eba064afea9cfb98aa842b405
출처 데이터셋: uspto-grants-1978_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04067720

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