Dichloromethane → HCID 22765685, 화합물
반응식
Cl.[CH2:2]([NH:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH:3]=[CH2:4].C(Cl)Cl.[Cl:13][CH:14]([Cl:18])[C:15](Cl)=[O:16]>C(N(CC)CC)C>[CH2:2]([N:5]([CH2:6][CH2:7][CH2:8][CH3:9])[C:15](=[O:16])[CH:14]([Cl:18])[Cl:13])[CH:3]=[CH2:4]참가 물질
5
실험 절차
Ten and five-tenths grams of allyl-n-butyl amine hydrochloride was added to 100 ml. of methylene chloride followed by 14.5 g. of triethylamine. The mixture was stirred in a water bath at room temperature while 10.4 g. of dichloroacetyl chloride was added dropwise, and stirring was continued for 30 minutes after addition was complete. The mixture was washed and the solvent stripped under vacuum. Yield was 13 g., nD30 1.4603. The intermediate was used without further purification to prepare Compound No. 12 (Example VII).
후처리
- stirringstirring
- additionafter addition
- washThe mixture was washed
- customThe intermediate was used without further purification
- customto prepare Compound No
출처 및 근거
- ORD 기록
- ord-c4f6d65782d343dfbad6f8dc53dc3ced
- 출처 데이터셋
- uspto-grants-1978_01
- 특허 번호
- US04069038
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