2-Amino-4-phenoxybutanoic acid → HCID 21713010, 화합물

HRID 1834836노트

반응식

HRID 1834836 반응식
[NH2:1][CH:2]([CH2:6][CH2:7][O:8][C:9]1[C:18]2[C:13](=CC=CC=2)[CH:12]=[CH:11][CH:10]=1)[C:3](O)=[O:4].NC(CCOC1C=CC=CC=1)C(O)=O>>[NH2:1][CH:2]([CH2:6][CH2:7][O:8][C:9]1[CH:18]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:3][OH:4]

참가 물질

3

반응물 2

HCID 131001282-Amino-4-phenoxybutanoic acidHCID 227550002-Amino-4-(1-naphthyloxy)butanoic acid

생성물 1

HCID 21713010HCID 21713010, 화합물

실험 절차

In the same manner but replacing 2-amino-4-(1-naphthyloxy)butanoic acid with an equivalent amount of 2-amino-4-phenoxy-butanoic acid, described by Y. Knobler, et al., J. Org. Chem., 24, 1794 (1959), 2-amino-4-phenoxy-1-butanol, γmaxCHCl3 3230-3400, is obtained. The hydrochloric acid addition salt of 2-amino-4-phenoxy-1-butanol has mp 136°-138° C, after recrystallization from methanol-diethyl ether.

출처 및 근거

ORD 기록
ord-a3ed44909cb24af1b2d1785e4b4bab3f
출처 데이터셋
uspto-grants-1978_01
특허 번호
US04071552

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