1-Iodononane → 6-Acetyl-4,4-dimethyl-1-nonyl-3,4-dihydroquinolin-2(1H)-one

반응식

[CH2:1]([N:7]1[C:16]2[C:11](=[CH:12][C:13]([C:17](=[O:19])[CH3:18])=[CH:14][CH:15]=2)[C:10]([CH3:21])([CH3:20])[CH2:9][C:8]1=[O:22])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].I[CH2:24][CH2:25][CH2:26]CCCCCC>>[CH2:1]([N:7]1[C:16]2[C:11](=[CH:12][C:13]([C:17](=[O:19])[CH3:18])=[CH:14][CH:15]=2)[C:10]([CH3:21])([CH3:20])[CH2:9][C:8]1=[O:22])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:24][CH2:25][CH3:26]

참가 물질

반응물 2

HCID 202751-Iodononane

HCID 121354162(1H)-Quinolinone, 6-acetyl-1-hexyl-3,4-dihydro-4,4-dimethyl-

생성물 1

HCID 234447006-Acetyl-4,4-dimethyl-1-nonyl-3,4-dihydroquinolin-2(1H)-one

실험 절차

Following a procedure similar to that used for the preparation of Intermediate 6a but using 1-iodo-n-nonane as the alkylating reagent the title compound was obtained as a colorless oil (70% yield).

출처 및 근거

ORD 기록: ord-6d93beeb9cb142329ec0c32b2b358192
출처 데이터셋: uspto-grants-2004_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06683092B1

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