Methyl 2-iodoisonicotinate → 2-(3,4-Dichloro-phenyl)-isonicotinic acid methyl ester

HRID 1841233

반응식

HRID 1841233 반응식
[CH3:1][O:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][N:7]=[C:6](I)[CH:5]=1.[Cl:12][C:13]1[CH:14]=[C:15](B(O)O)[CH:16]=[CH:17][C:18]=1[Cl:19]>>[CH3:1][O:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][N:7]=[C:6]([C:16]2[CH:15]=[CH:14][C:13]([Cl:12])=[C:18]([Cl:19])[CH:17]=2)[CH:5]=1

참가 물질

3

반응물 2

HCID 196869Methyl 2-iodoisonicotinateHCID 27343303,4-Dichlorobenzeneboronic acid

생성물 1

HCID 690406242-(3,4-Dichloro-phenyl)-isonicotinic acid methyl ester

실험 절차

The title compound, MS: m/e=281.0 (M+) was obtained as a light brown solid (59% yield) by the reaction of 2-iodo-isonicotinic acid methyl ester with 3,4-dichlorophenyl boronic acid.

출처 및 근거

ORD 기록
ord-fb080892b52a4f2aa8765f10d30914af
출처 데이터셋
uspto-grants-2004_01
특허 번호
US06683097B2

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