Phenyl N-(5,6-dimethyl-2-methoxypyrazin-3-yl)carbamate → 1-[(5,6-Dimethyl-2-methoxypyrazin-3-yl)aminocarbonyl]-4-(3,5-dinitrophenyl)piperazine

HRID 1841459노트

반응식

HRID 1841459 반응식
[CH3:1][C:2]1[N:3]=[C:4]([NH:11][C:12](=[O:20])OC2C=CC=CC=2)[C:5]([O:9][CH3:10])=[N:6][C:7]=1[CH3:8].[N+:21]([C:24]1[CH:25]=[C:26]([N:33]2[CH2:38][CH2:37][NH:36][CH2:35][CH2:34]2)[CH:27]=[C:28]([N+:30]([O-:32])=[O:31])[CH:29]=1)([O-:23])=[O:22]>>[CH3:1][C:2]1[N:3]=[C:4]([NH:11][C:12]([N:36]2[CH2:37][CH2:38][N:33]([C:26]3[CH:27]=[C:28]([N+:30]([O-:32])=[O:31])[CH:29]=[C:24]([N+:21]([O-:23])=[O:22])[CH:25]=3)[CH2:34][CH2:35]2)=[O:20])[C:5]([O:9][CH3:10])=[N:6][C:7]=1[CH3:8]

참가 물질

3

반응물 2

HCID 11173351Phenyl N-(5,6-dimethyl-2-methoxypyrazin-3-yl)carbamateHCID 234463481-(3,5-Dinitrophenyl)piperazine

생성물 1

HCID 234461841-[(5,6-Dimethyl-2-methoxypyrazin-3-yl)aminocarbonyl]-4-(3,5-dinitrophenyl)piperazine수율 64.5%

실험 절차

Phenyl N-(5,6-dimethyl-2-methoxypyrazin-3-yl)carbamate and 1-(3,5-dinitrophenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

출처 및 근거

ORD 기록
ord-5802ddc2132949cfb56a72f1db33badd
출처 데이터셋
uspto-grants-2004_01
특허 번호
US06683184B2

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