1-(4-Butylphenyl)piperazine → 1-[(2-Methoxyquinoxalin-3-yl)aminothiocarbonyl]-4-(4-but-ylphenyl) piperazine

HRID 1841494노트

반응식

HRID 1841494 반응식
[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14](=[S:22])OC2C=CC=CC=2)=[N:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1.[CH2:23]([C:27]1[CH:32]=[CH:31][C:30]([N:33]2[CH2:38][CH2:37][NH:36][CH2:35][CH2:34]2)=[CH:29][CH:28]=1)[CH2:24][CH2:25][CH3:26]>>[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14]([N:36]2[CH2:37][CH2:38][N:33]([C:30]3[CH:31]=[CH:32][C:27]([CH2:23][CH2:24][CH2:25][CH3:26])=[CH:28][CH:29]=3)[CH2:34][CH2:35]2)=[S:22])=[N:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1

참가 물질

3

반응물 2

HCID 46155681-(4-Butylphenyl)piperazineHCID 53676590Phenyl N-(2-methoxyquinoxalin-3-yl)thiocarbamate

생성물 1

HCID 234463231-[(2-Methoxyquinoxalin-3-yl)aminothiocarbonyl]-4-(4-but-ylphenyl) piperazine수율 62.5%

실험 절차

Phenyl N-(2-methoxyquinoxalin-3-yl)thiocarbamate and 1-(4-butylphenyl)piperazine were reacted by the same way with the example 63 to obtain the titled compound.

출처 및 근거

ORD 기록
ord-a9459e2ddec14b5290a21a9af8992822
출처 데이터셋
uspto-grants-2004_01
특허 번호
US06683184B2

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