HCID 86158515, 화합물 → HCID 19372161, 화합물

HRID 1841873노트

반응식

HRID 1841873 반응식
[CH3:1][O:2][C:3](=[O:22])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][N:19]=[N+]=[N-]>CO.[Pd]>[CH3:1][O:2][C:3](=[O:22])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][NH2:19]

참가 물질

4

반응물 1

HCID 86158515HCID 86158515, 화합물

생성물 1

HCID 19372161HCID 19372161, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

16-azidohexadecanoic acid methyl ester is catalytically hydrogenated with palladium/activated charcoal in methanol at 3 bar for three hours to give the corresponding amine (Zinic et al., Positionally Isomeric Organic Gelators: Structure-Gelation Study, Racemic versus Enantiomeric Gelators, and Solvation Effects, Chem. Eur. J. 2010; 16:3066-82).

출처 및 근거

ORD 기록
ord-4e127cdbee584fd48a1f74d53939a02e
출처 데이터셋
uspto-grants-2015_02
특허 번호
US08945897B2

반응 노트

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