Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 2,4,5-Trifluoro-3-methoxybenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2,4,5-Trifluoro-3-methoxybenzoic acid | HCID 2733970 | — |
| 생성물 | 2,4,5-Trifluoro-3-methoxybenzoyl chloride | HCID 2775281 | — |
반응 단계
A mixture of 2,4,5-trifluoro-3-methoxybenzoic acid (154 mg, 0.75 mmol) and thionyl chloride (8 mL) is refluxed for 4 h. Excess thionyl chloride is removed in vacuo, and the remaining residue is used directly in the next synthetic step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08946422B2 |
| 출처 데이터셋 | uspto-grants-2015_02 |
| ORD ID | ord-d8bd22cc7a604f0ea2f8c25d160b063b |
| 출처 메모 | uspto-grants-2015_02 |