Cyclohexanemethylamine → HCID 86719133, 화합물
반응식
[C:1]([C:5]1[CH:6]=[C:7]([C:15](=O)[CH2:16][CH2:17][C:18](=O)[CH3:19])[CH:8]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:10]=1)([CH3:4])([CH3:3])[CH3:2].[CH:22]1([CH2:28][NH2:29])[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1>C1(C)C=CC=CC=1.CC1C=CC(S(O)(=O)=O)=CC=1>[CH:22]1([CH2:28][N:29]2[C:18]([CH3:19])=[CH:17][CH:16]=[C:15]2[C:7]2[CH:6]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:8]=2)[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1참가 물질
5
실험 절차
To a solution of 5a (6.4 g, 22.2 mmol) in toluene (100 mL) was added cyclohexylmethanamine (2.8 g, 24.4 mmol) and TsOH (0.3 g). This mixture was refluxed for 20 h, cooled, concentrated and purified by CC to afford compound 5b (7.5 g, 93%) as yellow oil.