Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trimethylsilylacetylene → N-benzoyl-4-ethynyl-3-nitrobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trimethylsilylacetylene | HCID 66111 | — |
| 반응물 | Trimethyl-2-propynylsilane | HCID 83378 | — |
| 반응물 | 4-Iodo-3-nitrobenzoic acid | HCID 11208598 | — |
| 반응물 | 4-iodo-N-methyl-3-nitrobenzamide | HCID 20755545 | — |
| 생성물 | N-benzoyl-4-ethynyl-3-nitrobenzamide | HCID 57331455 | — |
반응 단계
Compound I-14, Compound I-15, Compound I-16, Compound I-17, Compound I-18, Compound I-19, Compound I-20, Compound I-21, Compound I-22, Compound I-23, Compound I-24 and Compound I-25 were prepared sequentially according to the methods of Example 14, Example 15 and Example 16, by selecting appropriate amines and trimethylsilylacetylene, using the Compound 4-iodo-3-nitrobenzoic acid (Compound VI-1) as starting material; Compound I-26 was prepared sequentially according to the methods of Example 15 and Example 16, using the compound N-methyl-4-iodo-3-nitrobenzamide (Compound VII-1) and trimethylpropargylsilane as starting materials:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08946478B2 |
| 출처 데이터셋 | uspto-grants-2015_02 |
| ORD ID | ord-5db980f8b4964d14b4ace38065301a1e |
| 출처 메모 | uspto-grants-2015_02 |