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2(3H)-Benzoxazolone, 6-hydroxy- → HCID 86663929, 화합물

HRID 1846510
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HRID 1846510 반응식
Cl[C:2]1[C:7]([C:8]#[N:9])=[CH:6][N:5]=[C:4]([Cl:10])[CH:3]=1.[OH:11][C:12]1[CH:21]=[CH:20][C:15]2[NH:16][C:17](=[O:19])[O:18][C:14]=2[CH:13]=1.[K].[CH3:23]C(C)([O-])C>CN1C(=O)CCC1>[Cl:10][C:4]1[CH:3]=[C:2]([O:11][C:12]2[CH:21]=[C:20]([CH3:23])[C:15]3[NH:16][C:17](=[O:19])[O:18][C:14]=3[CH:13]=2)[C:7]([C:8]#[N:9])=[CH:6][N:5]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 1571672(3H)-Benzoxazolone, 6-hydroxy-HCID 455880804,6-Dichloropyridine-3-carbonitrileHCID 50987170Potassium tertbutoxide

생성물 1

HCID 86663929HCID 86663929, 화합물

시약·촉매·용매 1

HCID 13387N-methyl-2-pyrrolidone용매

실험 절차

0.12 g (0.69 mmol) 4,6-dichloro-nicotinonitrile, 0.15 g (0.91 mmol) 6-hydroxy-2-benzoxazolinone and 90 mg (0.80 mmol) potassium-tert.-butoxide in 0.8 mL NMP were stirred for 2 h at 70° C. The reaction mixture was combined with ice water. The precipitate formed was suction filtered and dried.

후처리

  1. customThe precipitate formed
  2. filtrationfiltered
  3. customdried

출처 및 근거

ORD 기록
ord-875d8bb8ab5e4364ac686f205b6d22df
출처 데이터셋
uspto-grants-2015_02
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08952014B2

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