Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 2-acetamidoacrylate → Methyl 6-methylisoquinoline-3-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 2-acetamidoacrylate | HCID 98644 | — |
| 반응물 | 2-Bromo-4-methylbenzaldehyde | HCID 4645292 | — |
| 생성물 | Methyl 6-methylisoquinoline-3-carboxylate | HCID 22243644 | 50% |
반응 단계
methyl 6-methyl-isoquinoline-3-carboxylate was prepared using the procedure described in example 12A: 2-bromo-4-methylbenzaldehyde was reacted with methyl 2-acetamidoacrylate at 110° C. for 18 hours to yield methyl 6-methyl-isoquinoline-3-carboxylate (50%) as brown solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08962627B2 |
| 출처 데이터셋 | uspto-grants-2015_02 |
| ORD ID | ord-ed8c84d3d8f7478eac387d95047051c1 |
| 출처 메모 | uspto-grants-2015_02 |