Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Divinyl sulfone → [4-(1,1-Dioxo-1lambda6-thiomorpholin-4-yl)-phenyl]-carbamic acid tert-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Divinyl sulfone | HCID 6496 | — |
| 반응물 | tert-Butyl (4-aminophenyl)carbamate | HCID 688611 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | [4-(1,1-Dioxo-1lambda6-thiomorpholin-4-yl)-phenyl]-carbamic acid tert-butyl ester | HCID 68616091 | — |
반응 단계
A solution of 408 mg (4-Amino-phenyl)-carbamic acid tert-butyl ester and 254 mg Ethenesulfonyl-ethene in 4 mL EtOH were heated for 30 min at 140° C. under microwave irradiation (100 W, CEM Discover™ apparatus). Then, after cooling to RT the solvents were removed under reduced pressure and the residue was dried in vacuo. The crude product was subjected to the next reaction step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741341B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-770f859b938246188dc93593dd1d1dc5 |
| 출처 메모 | uspto-grants-2010_06 |