Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butoxy bis(dimethylamino)methane → Ethyl 3-dimethylamino-2-(4-trifluoromethyl-benzoyl)-acrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| 반응물 | Ethyl 3-oxo-3-(4-(trifluoromethyl)phenyl)propanoate | HCID 2760281 | — |
| 생성물 | Ethyl 3-dimethylamino-2-(4-trifluoromethyl-benzoyl)-acrylate | HCID 54156258 | — |
반응 단계
Ethyl 3-oxo-3-(4-trifluoromethyl-phenyl)-propionate (130 mg, 0.5 mmol) was reacted with tert.-butoxy-bis-(dimethylamino)-methane using in analogous manner the procedure described in example 28a) to give crude title compound (151 mg) as a red oil which was used directly in the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08962834B2 |
| 출처 데이터셋 | uspto-grants-2015_02 |
| ORD ID | ord-f9708dd493ec47e3ac8f58fca8d358b2 |
| 출처 메모 | uspto-grants-2015_02 |