tert-Butoxy bis(dimethylamino)methane → HCID 68632008, 화합물

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[CH3:1][C:2]1[N:6]=[C:5]([CH2:7][C:8](=[O:10])[CH3:9])[O:4][N:3]=1.C(O[CH:16](N(C)C)[N:17]([CH3:19])[CH3:18])(C)(C)C>>[CH3:16][N:17]([CH3:19])[CH:18]=[C:7]([C:5]1[O:4][N:3]=[C:2]([CH3:1])[N:6]=1)[C:8](=[O:10])[CH3:9]

참가 물질

반응물 2

HCID 79885tert-Butoxy bis(dimethylamino)methane

HCID 129553831-(3-Methyl-1,2,4-oxadiazol-5-yl)acetone

생성물 1

HCID 68632008HCID 68632008, 화합물

실험 절차

1-(3-Methyl-[1,2,4]oxadiazol-5-yl)-propan-2-one (224 mg, 1.6 mmol) was reacted with tert.-butoxy-bis-(dimethylamino)-methane using in analogous manner the procedure described in example 28a) to give crude title compound (313 mg) as a yellow oil which was used directly in the next step.

출처 및 근거

ORD 기록: ord-6d7dc51192914be8a9db0cd507fa96fe
출처 데이터셋: uspto-grants-2015_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08962834B2

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