Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diisopropylamine → N,N"-(1,4-Phenylene)bis[N',N'-bis(1-methylethyl)thiourea]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diisopropylamine | HCID 7912 | — |
| 반응물 | p-Phenylene diisothiocyanate | HCID 19958 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N,N"-(1,4-Phenylene)bis[N',N'-bis(1-methylethyl)thiourea] | HCID 23346036 | — |
반응 단계
To a solution of 1.92 g. of 1,4-phenylenediisothiocyanate in 100 ml. of acetonitrile is added 2.5 g. of diisopropylamine. On standing, a precipitate forms which is filtered off and crystallized from acetone-cyclohexane to yield 2.7 g. of the title compound, melting point 185° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04218396 |
| 출처 데이터셋 | uspto-grants-1980_08 |
| ORD ID | ord-eb2cf8b6e22245c39b51d070cdc91d54 |
| 출처 메모 | uspto-grants-1980_08 |