HCID 12769229, 화합물 → HCID 21163102, 화합물

HRID 1856248노트

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HRID 1856248 반응식
[N:1]([CH:4]1[C:11](=[O:12])[N:10]2[CH:5]1[CH2:6][CH2:7]OC2(C)C)=[N+:2]=[N-:3].O=C1N2C(CCOC2(C)C)C1.[Si:26](N1C(C=C)CC1=O)([C:29]([CH3:32])([CH3:31])[CH3:30])([CH3:28])[CH3:27]>>[Si:26]([N:10]1[CH:5]([CH:6]=[CH2:7])[CH:4]([N:1]=[N+:2]=[N-:3])[C:11]1=[O:12])([C:29]([CH3:32])([CH3:31])[CH3:30])([CH3:28])[CH3:27]

참가 물질

4

반응물 3

HCID 12769229HCID 12769229, 화합물HCID 12769232HCID 12769232, 화합물HCID 140681691-(t-Butyldimethylsilyl)-4-vinyl-2-azetidinone

생성물 1

HCID 21163102HCID 21163102, 화합물

실험 절차

Following the procedure described for the preparation of 7-azido-8-oxo-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]-octane from 8-oxo-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]-octane (Example 5, Step A) and using 1-(t-butyldimethylsilyl)-4-vinyl-2-azetidinone there is obtained 1-(t-butyldimethylsilyl)-3-azido-4-vinyl-2-azetidinone.

출처 및 근거

ORD 기록
ord-3a4546113a3945a1ab964928e9d70900
출처 데이터셋
uspto-grants-1980_08
특허 번호
US04218463

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