(4-Methoxyphenyl)(naphthalen-2-yl)methanone → HCID 15640646, 화합물
반응식
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]([C:13]1[CH:18]=[CH:17][C:16]([O:19]C)=[CH:15][CH:14]=1)=[O:12].C[S-].[Na+]>CN(C)C=O>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]([C:13]1[CH:14]=[CH:15][C:16]([OH:19])=[CH:17][CH:18]=1)=[O:12]참가 물질
4
실험 절차
4-Methoxyphenyl 2-naphthyl ketone (735 mg) obtained in Example 35 was dissolved in N,N-dimethylformamide (20 ml), sodium thiomethoxide (491 mg) was added, and the admixture was refluxed under argon for 5 hours. The reaction mixture was treated in the same manner as described in Example 33 to obtain 595 mg of the title compound (yield: 86%).
후처리
- temperaturethe admixture was refluxed under argon for 5 hours
- additionThe reaction mixture was treated in the same manner
출처 및 근거
- ORD 기록
- ord-0b6e6f7945f146d7a0d08b4d122512c5
- 출처 데이터셋
- uspto-grants-2000_11
- 특허 번호
- US06143764
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