Hydroquinone → tert-Butyl peroxybenzoate

HRID 1858054

반응식

HRID 1858054 반응식
C[O-].[Na+].[O-2].[Al+3].[O-2].[O-2].[Al+3].C1(C=CC(O)=CC=1)[OH:10].CCC(OOC(OO)(CC)C)(OO)C.CN(C)C1C=CC=CC=1.[C:40]([O:49][O:50][C:51]([C:54]1[CH:59]=[CH:58][CH:57]=[CH:56][CH:55]=1)(C)C)([C:43]1C=CC=CC=1)([CH3:42])[CH3:41].C(OCCOCCOC(=O)C=C)(=O)C=C>ClCCl.C1(C)C=CC=CC=1>[C:40]([O:49][O:50][C:51](=[O:10])[C:54]1[CH:59]=[CH:58][CH:57]=[CH:56][CH:55]=1)([CH3:43])([CH3:42])[CH3:41]

참가 물질

10

반응물 7

HCID 785HydroquinoneHCID 949N,N-DimethylanilineHCID 6641Dicumyl peroxideHCID 19996Diethylene glycol diacrylateHCID 3672772Methyl ethyl ketone peroxideHCID 9989226AluminaHCID 10942334Sodium Methoxide

생성물 1

HCID 11966tert-Butyl peroxybenzoate

시약·촉매·용매 2

HCID 1140Toluene용매HCID 6344Dichloromethane용매

실험 절차

Sodium methoxide (NaOCH3), toluene (anhydrous), dichloromethane, hexanes, activated neutral aluminum oxide (60 to 50 mesh), hydroquinone, methyl ethyl ketone peroxide, dimethylaniline, dicumylperoxide, diethylene glycol diacrylate, and tert-butylperoxybenzoate were obtained from commercial sources and used as received.

출처 및 근거

ORD 기록
ord-1b265212be2f48a2b206a49a2742bb59
출처 데이터셋
uspto-grants-2000_11
특허 번호
US06150429

연결된 노트

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