Sulfuric Acid → HCID 18625136, 화합물

HRID 1859369노트

반응식

[C:1]([N:14]([CH3:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].S(=O)(=O)(O)O.[CH:26](O)([CH3:28])[CH3:27]>>[CH:26]([O:18][C:17](=[O:19])[CH2:16][CH2:15][N:14]([C:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:20])([CH3:28])[CH3:27]

참가 물질

반응물 3

HCID 1118Sulfuric Acid

HCID 3776Isopropanol

HCID 9818053Lauroyl methyl beta-alanine

생성물 1

HCID 18625136HCID 18625136, 화합물

실험 절차

One hundred grams(100) of N-lauroyl-N-methyl-β-alanine and 750 ml of isopropanol were charged into a 1,000-milliliter flask. Further, 2 ml of conc. sulfuric acid were added as the catalyst. The mixture was heated under ref lux for reaction for 8 hours.

후처리

temperatureThe mixture was heated under ref lux for reaction for 8 hours

출처 및 근거

ORD 기록: ord-3996145788194df08bb625b2f0a17974
출처 데이터셋: uspto-grants-2003_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06528068B1

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