Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → 3-Amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 3,4-Dichloroaniline | HCID 7257 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 4-Methoxy-3-nitrobenzoic acid | HCID 66640 | — |
| 생성물 | 3-Amino-4-methoxy-N-(3,4-dichlorophenyl)-benzamide | HCID 9948627 | 68.5% |
반응 단계
Prepared according to the procedure described for Example 1 using oxalyl chloride (5.0 mL, 57.31 mmol), 3-nitro-4-methoxybenzoic acid (5.04 g, 25.56 mmol), dimethylformamide (0.5 mL, 6.46 mmol), and 3,4-dichloroaniline (8.3 g, 51 mmol) to afford the product (5.45 g); m.p. 179-182° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06528528B2 |
| 출처 데이터셋 | uspto-grants-2003_03 |
| ORD ID | ord-2a0a0dec0107459a956d91f04badc95f |
| 출처 메모 | uspto-grants-2003_03 |