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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1863143생성일: 2026년 10월 27일

Ethyl red → Benzopinacol

https://huagongshe.com/reaction/1863143

반응식

참여 물질

역할이름HCID투입량
반응물Ethyl redHCID 54832—
반응물Ethyl red iodideHCID 5463397—
반응물1,2-Diphenyl-1,2-bis(2,3,5,6-tetrafluoro-4-methoxyphenyl)-1,2-ethanediolHCID 54301795—
용매Methylcellosolve-acetonHCID 18314300—
생성물BenzopinacolHCID 94766—

반응 조건

온도160 °C

반응 단계

Ethyl red (2.0 mg), 1,1'-diethyl-2,4'-cyanine iodide, was dissolved in 2.0 ml. of acetone/2-methoxyethanol. Then, 50 mg of 4,4"-dimethoxy-2,3,5,6,2",3",5",6"-octafluorobenzopinacol was added. The solution was mixed with 1.0 ml of 20 percent polysulfonamide polymer solution (acetone/2-methoxyethanol (1:1)). The solution was mixed and coated on poly(ethylene terephthalate) film base at a wet thickness of 0.098 mm. It was allowed to dry at 49° C. for 15 minutes. The dye in the film had λ max at 565 nm, and at 530 nm, the optical density was 1.8 and 0.93, respectively. The film was heated at 160° C. for 10 seconds. The optical density of the heated film was 0.20 at λ=565 and 0.18 at 530 nm. The reduction in the dye density was 89 percent and 81 percent, at the two wavelengths. The same results were obtained after the film had been held in storage at room temperature for 6 months.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04168218
출처 데이터셋uspto-grants-1979_09
ORD IDord-62f854ceafea47529baaa1c1e99ca39e
출처 메모uspto-grants-1979_09