참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylcarbamoyl Chloride | HCID 6598 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | HCID 178429033 | HCID 178429033 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Carbamic acid, dimethyl-, 2,6-dimethyl-4-pyridinyl ester | HCID 19112 | — |
반응 단계
30,8 g (0,25 mole) of 2,6-dimethyl-4-hydroxypyridine were suspended in 500 ml of acetonitrile, 69 g (0,5 mole) of potassium carbonate were added and the mixture was heated to reflux temperature for 2 hours. Subsequently 47 g (0,44 mole) of dimethylcarbamic acid chloride were added at an interior temperature of approximately 60°-70° C. and the mixture was maintained for two hours at about 80° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04168311 |
|---|
| 출처 데이터셋 | uspto-grants-1979_09 |
|---|
| ORD ID | ord-0d7f368c27a0473eb24cf27cb4e322ef |
|---|
| 출처 메모 | uspto-grants-1979_09 |
|---|
