Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfanilamide → 4-(2-Methyl-5-m-tolyl-pyrrol-1-yl)-benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfanilamide | HCID 5333 | — |
| 반응물 | Methyl vinyl ketone | HCID 6570 | — |
| 반응물 | 3-Methylbenzaldehyde | HCID 12105 | — |
| 생성물 | 4-(2-Methyl-5-m-tolyl-pyrrol-1-yl)-benzenesulfonamide | HCID 68484259 | — |
반응 단계
Meta-methylbenzaldehyde and but-3-en-2-one were treated according to the procedure outlined in General Procedure C followed by subjecting the resulting product to conditions outlined in General Procedure D along with p-aminosulfonyl phenylamine to obtain the titled compound. 1H NMR (CDCl3) δ ppm 2.15 (3H), 2.05 (3H), 4.90 (2H), 6.10 (1H), 6.30 (1H), 6.89-7.90 (8H); MS (ESI) m/z 327 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741364B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-5c2fa4e2b03541a59abf59fc72cb1df7 |
| 출처 메모 | uspto-grants-2010_06 |