Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → Methyl 3-methyl-2-nitrobenzenecarboximidate tetrafloroborate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| 반응물 | 3-Methyl-2-nitrobenzamide | HCID 3271371 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Methyl 3-methyl-2-nitrobenzenecarboximidate tetrafloroborate | HCID 17960598 | 102.5% |
반응 단계
To a solution of the title compound of Step A (1.07 g, 5.9 mmol) in dichloromethane (15 mL) was added trimethyloxonium tetrafluoroborate (1.06 g, 7.1 mmol) and the mixture was stirred overnight at ambient temperature. Concentration gave the title compound of Step B as a white solid (1.7 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07629463B2 |
| 출처 데이터셋 | uspto-grants-2009_12 |
| ORD ID | ord-265cd94fda2c4fd99182acf864724307 |
| 출처 메모 | uspto-grants-2009_12 |